By contrast, solid state nmr spectra are very broad, as the full effects of anisotropic or orientationdependent interactions are observed in the spectrum. Introduction to solidstate nmr spectroscopy, melinda j. Mar 17, 2014 discover book depositorys huge selection of solid state chemistry books online. Solid state nmr spectroscopy is a powerful method in many research areas.
Introduction to solidstate nmr spectroscopy melinda. International edition isbn number and front cover may be different in rare cases but contents are same as the us edition. The book cover links to the publishers website, however copies of this book are available for a cheaper price on other websites. Basic principles, concepts and applications in chemistry by harald gunther.
Introduction to solidstate nmr spectroscopy duer, melinda j. Introduction to solidstate nmr spectroscopy by duer, melinda j. Duer nmr lineshapes and lineshape fitting procedures john higinbotham and ian marshall recent progress in solidstate nmr of lowy. A solidstate nmr investigation of the oddeven effect in. The main structural characterization technique we use to study molecular structure in tissues is solidstate nuclear magnetic resonance nmr spectroscopy. Her work focuses on studying the structure and dynamics of healthy and glycated extracellular matrix collagen using solid state nmr spectroscopy. Annual reports on nmr spectroscopy, volume 43 1st edition. This dual requirement is met through careful construction of. Solidstate nmr studies of molecular motion melinda j. Melinda duer is a lecturer in the department of chemistry, university of cambridge and has worked in the field of solidstate nmr spectroscopy for more than ten years. This nonequilibrium magnetization can be induced, generally by applying a pulse of radiofrequency close to the larmor frequency of the nuclear spins. Compared to the more common solution nmr spectroscopy, ssnmr usually requires additional hardware for highpower radiofrequency irradiation and magicangle spinning. The theory of solidstate nmr and its experiments, 1 1 the basics of solidstate nmr, 3 melinda j. State nmr spectroscopy principles and applications.
By contrast, solidstate nmr spectra are very broad, as the full effects of anisotropic or orientationdependent interactions are observed in the spectrum. Books and hand books dealing with solid state nmr and quadrupole nuclei with halfinteger spin. Highresolution solidstate mas nmr 2 1cos3 2 q rotor with sample in the rf coil zr rot. The main structural characterization technique we use to study molecular structure in tissues is solid state nuclear magnetic resonance nmr spectroscopy. Especially helpful if you wish to get familiarized with averaged hamiltonian theory. This includes advances in instrumentation, development of new experimental techniques and methodology, new theoretical insights, new data processing and simulation. Batteries in semiordered or ordered materials, such as batteries, important transport processes can be measured. In fourier transform nuclear magnetic resonance spectroscopy, free induction decay fid is the observable nmr signal generated by nonequilibrium nuclear spin magnetization precessing about the magnetic field conventionally along z. A recent project has used 17 o nmr to study the dynamics of oxygen motion in zrw 2 o 8.
The term nmr crystallography has only recently come into common usage, and even now causes raised eyebrows within some parts of the diffraction community. This book is for those familiar with solutionstate nmr who are encountering solidstate nmr for the first time. Everyday low prices and free delivery on eligible orders. Dr melinda duer is a senior lecturer in the department of chemistry at the university of cambridge, cambridge, uk. Solid state nmr spectroscopy, by melinda duer 2005 middle level publisher webpage for this bookthis is a good middle level book on a number of ssnmr topics, with a detail level that works well for a 23 year graduate student. The principal values of the c chemical shift tensor for both benzene and hexafluorobenzene components are found to be very similar to those. We use 2d and 3d c and 15 n nmr to study molecular structure in native tissues and in in vitro tissues. With its basic, simple, and clear treatment of math and terminology this book is an excellent overview for the first year graduate.
It presents the current understanding and applications of solidstate nmr with a rigorous but readable approach, making it easy for someone who merely wishes to gain an overall impression of the subject without details. Introduction to solid state nmr spectroscopy is written for undergraduate and graduate students of chemistry, either taking a course in advanced or solidstate nuclear magnetic resonance spectroscopy or undertaking research projects where solidstate nmr is likely to be a major. Duer, 97806320535, available at book depository with free delivery worldwide. About the author melinda duer is a lecturer in the department of chemistry, university of cambridge and has worked in the field of solidstate nmr spectroscopy for more than ten years. Find introduction to solid state nmr spectroscopy by duer, melinda j at biblio. Nmr crystallography the content of this volume has been added to emagres formerly encyclopedia of magnetic resonance the ultimate online resource for nmr and mri. Solid state nmr spectroscopy, by melinda duer 2005 middle level publisher webpage for this book this is a good middle level book on a number of ssnmr topics, with a detail level that works well for a 23 year graduate student. Solidstate c and 2h nuclear magnetic resonance studies of. Solidstate c and 2h nuclear magnetic resonance studies. Solidstate nmr ssnmr spectroscopy is a special type of nuclear magnetic resonance nmr spectroscopy, characterized by the presence of anisotropic directionally dependent interactions. Introduction to solidstate nmr spectroscopy by melinda j. Dec 21, 2001 melinda duer is a lecturer in the department of chemistry, university of cambridge and has worked in the field of solid state nmr spectroscopy for more than ten years. Discover book depositorys huge selection of solid state chemistry books online. Buy introduction to solidstate nmr spectroscopy book online.
Books and handbooks dealing with solid state nmr and quadrupole nuclei with halfinteger spin. Collagen structurefunction relationships from solidstate. It presents the current understanding and applications of solid state nmr with a rigorous but readable approach, making it easy for someone who merely wishes to gain an overall impression of the subject without details. Uncommonly good collectible and rare books from uncommonly good booksellers. Solid state nuclear magnetic resonance journal elsevier. The molecules consist of a flexible alkyl chain ch2n, with identical aromatic mesogenic groups at either end. It presents the current understanding and applications of solid state nmr with a rigorous but readable approach, making it easy for someone who merely. Introduction to solid state nmr spectroscopy edition 1. Her work focuses on studying the structure and dynamics of healthy and glycated extracellular matrix collagen using solidstate nmr spectroscopy. We are currently exploring how solidstate nmr, powder xrd and first principles calculations can be fully integrated to solve increasingly complex.
The journal solid state nuclear magnetic resonance publishes original manuscripts of high scientific quality dealing with all experimental and theoretical aspects of solid state nmr. Introduction to solidstate nmr spectroscopy edition 1 by. A introductory level book that illuminates the basic principles of spin interactions and their manipulation in solidstate nmr. Compared to the more common solution nmr spectroscopy, ssnmr usually requires additional hardware for highpower radiofrequency irradiation and magicangle. Measuring the charge transport in batteries can help understand the reason for its conductivity. Buy introduction to solidstate nmr spectroscopy book online at best prices in india on. Solidstate nmr spectroscopy principles and applications. Emsley university of southampton southampton uk george a. Find introduction to solidstate nmr spectroscopy by duer, melinda j at biblio. The ampere biological solidstate nmr school is a course intended for ph. Duer university of cambridge cambridge uk bernard c. Compared to the more common solution nmr spectroscopy, ssnmr usually requires additional hardware for highpower radiofrequency irradiation and magic. The origin of the oddeven effect in the solidnematic phase transition temperatures for a series of molecules is investigated by a variety of solidstate nmr experiments and powder xrd.
Solid state nmr ssnmr spectroscopy is a special type of nuclear magnetic resonance nmr spectroscopy, characterized by the presence of anisotropic directionally dependent interactions. We also apply the relatively new methodology of nmr crystallography, a combination. Enter your mobile number or email address below and well send you a link to download the free kindle app. Compared to the more common solution nmr spectroscopy, ssnmr usually requires additional hardware for high. Basic principles and practice by david c apperley, robin k harris, paul hodgkinson isbn. Introduction to solidstate nmr spectroscopy by duer.
With additional coverage of the practical implementation of solidstate nmr experiments integrated into the discussion, this book will be essential reading for all those using, or about to use, solidstate nmr spectroscopy. A introductory level book that illuminates the basic principles of spin interactions and their manipulation in solid state nmr. A practical introduction volume 1, david e axelson. Introduction to solid state nmr spectroscopy is written for undergraduate and graduate students of chemistry, either taking a course in advanced or solidstate nuclear magnetic resonance spectroscopy or undertaking research projects where solidstate nmr is likely to be a major investigative technique. Stanford libraries official online search tool for books, media, journals, databases, government documents and more.
The power of solidstate nmr to give crystallographic information has considerably increased since the cpmas suite of techniques was introduced in 1976. Ernst, geoffrey bodenhausen, alexander wokaun introduction to solidstate nmr spectroscopy by melinda j. Buy introduction to solidstate nmr spectroscopy book. It presents the current understanding and applications of solidstate nmr with a. Buy introduction to solid state nmr spectroscopy book online at best prices in india on. With additional coverage of the practical implementation of solid state nmr experiments integrated into the discussion, this book will be essential reading for all those using, or about to use, solid state nmr spectroscopy. Morris university of manchester manchester uk biochemical nmr ann e.
Introduction to solidstate nmr spectroscopy edition 1. Oct 23, 2001 melinda duer is a lecturer in the department of chemistry, university of cambridge and has worked in the field of solid state nmr spectroscopy for more than ten years. John evans, we apply solid state nmr of the study of inorganic framework materials characterisation of the structure of these materials by powder diffraction techniques alone is difficult, but combining the local information on structure and dynamics from multinuclear nmr e. Introduction to solid state nmr spectroscopy is written for undergraduate and graduate students of chemistry, either taking a course in advanced or solid state nuclear magnetic resonance spectroscopy or undertaking research projects where solid state nmr is likely to be a major. Click and collect from your local waterstones or get free uk delivery on orders over.
The school is focused on theoretical and experimental aspects of solidstate nmr applied to biomolecules. This book is for those familiar with solution state nmr who are encountering solid state nmr for the first time. Introduction to solid state nmr in solution nmr, spectra consist of a series of very sharp transitions, due to averaging of anisotropic nmr interactions by rapid random tumbling. A solidstate nmr c31p redor study reveals details of the structure of the protein. Free induction decay fid nuclear magnetic resonance signal seen from a well shimmed sample. Solidstate nmr spectroscopy magicangle spinning nmr spectroscopy on 1h, c, and 29si nuclei in the functionalized mesoporous proton conducting materials was performed in the fields of 9. Introduction to solid state nmr spectroscopy is written for undergraduate and graduate students of chemistry, either taking a course in advanced or solid state nuclear magnetic resonance spectroscopy or undertaking research projects where solid state nmr is likely to be a major investigative technique.
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